Structures by: Jing S.
Total: 82
C40H29IrN7O4P,0.17(C6H24O6)
C40H29IrN7O4P,0.17(C6H24O6)
Inorganica Chimica Acta (2014) 409B, 372-378
a=17.1230(14)Å b=12.2162(14)Å c=38.296(4)Å
α=90.00° β=102.815(2)° γ=90.00°
C41H29IrN5O4PS,2(CHCl3)
C41H29IrN5O4PS,2(CHCl3)
Inorganica Chimica Acta (2014) 409B, 372-378
a=12.1294(10)Å b=14.2619(12)Å c=14.6503(13)Å
α=85.8580(10)° β=79.7080(10)° γ=66.3920(10)°
C41H29IrN5O5P,2(CHCl3)
C41H29IrN5O5P,2(CHCl3)
Inorganica Chimica Acta (2014) 409B, 372-378
a=11.823(3)Å b=12.656(3)Å c=17.343(4)Å
α=85.868(3)° β=74.196(3)° γ=65.607(3)°
C14H10O2
C14H10O2
The journal of physical chemistry. B (2011) 115, 13 3588-3603
a=8.1037(16)Å b=10.127(2)Å c=12.519(3)Å
α=90.00° β=90.00° γ=90.00°
C29H26F12GdN5NiO10,H2O
C29H26F12GdN5NiO10,H2O
New J. Chem. (2015) 39, 5 3467
a=18.351(3)Å b=10.8682(15)Å c=19.911(3)Å
α=90° β=106.184(2)° γ=90°
C29H26F12N5NiO10Tb,H2O
C29H26F12N5NiO10Tb,H2O
New J. Chem. (2015) 39, 5 3467
a=17.8821(14)Å b=10.8892(11)Å c=20.0534(18)Å
α=90° β=106.038(2)° γ=90°
C22H24GdN7NiO15
C22H24GdN7NiO15
New J. Chem. (2015) 39, 11 8356
a=10.3265(19)Å b=17.115(3)Å c=17.194(3)Å
α=90° β=96.575(3)° γ=90°
C22H24N7NiO15Tb
C22H24N7NiO15Tb
New J. Chem. (2015) 39, 11 8356
a=10.309(3)Å b=17.095(5)Å c=17.232(5)Å
α=90° β=96.548(4)° γ=90°
C23H32N5NiO17Tb
C23H32N5NiO17Tb
New J. Chem. (2015) 39, 11 8356
a=10.0281(14)Å b=12.0551(17)Å c=15.254(2)Å
α=71.779(2)° β=86.572(2)° γ=68.175(2)°
C23H32DyN5NiO17
C23H32DyN5NiO17
New J. Chem. (2015) 39, 11 8356
a=10.0241(17)Å b=12.042(2)Å c=15.270(3)Å
α=71.869(2)° β=86.592(3)° γ=68.157(2)°
C22H24DyN7NiO15
C22H24DyN7NiO15
New J. Chem. (2015) 39, 11 8356
a=21.577(3)Å b=9.4531(12)Å c=15.866(2)Å
α=90° β=114.880(2)° γ=90°
C18H19CoN5O4
C18H19CoN5O4
CrystEngComm (2012) 14, 13 4478
a=9.2705(5)Å b=9.7701(5)Å c=11.4534(6)Å
α=72.8870(10)° β=80.2130(9)° γ=64.0520(10)°
C13H12CoN3O4
C13H12CoN3O4
CrystEngComm (2012) 14, 13 4478
a=11.0663(5)Å b=7.6170(3)Å c=16.0392(7)Å
α=90.00° β=91.7540(10)° γ=90.00°
C22H21CoN5O5
C22H21CoN5O5
CrystEngComm (2012) 14, 13 4478
a=10.195(2)Å b=10.242(5)Å c=12.011(2)Å
α=100.37(4)° β=95.68(3)° γ=115.82(2)°
C37H31Co2N8O8
C37H31Co2N8O8
CrystEngComm (2012) 14, 13 4478
a=10.7631(4)Å b=11.1927(4)Å c=15.5583(6)Å
α=107.1090(10)° β=95.3050(9)° γ=99.1550(10)°
C23H24Fe2Se2
C23H24Fe2Se2
Dalton transactions (Cambridge, England : 2003) (2006) 36 4335-4342
a=5.875(1)Å b=12.077(2)Å c=15.905(2)Å
α=108.13(1)° β=94.07(1)° γ=92.25(1)°
C23H24Fe2Pd0.50Se2,F6P1,C2H3N
C23H24Fe2Pd0.50Se2,F6P1,C2H3N
Dalton transactions (Cambridge, England : 2003) (2006) 36 4335-4342
a=10.8970(10)Å b=11.5410(10)Å c=11.7510(10)Å
α=78.950(10)° β=72.880(10)° γ=86.510(10)°
C23H24Fe2Pt0.50Se2,F6P1,C2H3N
C23H24Fe2Pt0.50Se2,F6P1,C2H3N
Dalton transactions (Cambridge, England : 2003) (2006) 36 4335-4342
a=10.8830(10)Å b=11.5380(10)Å c=11.752(2)Å
α=78.690(10)° β=72.750(10)° γ=86.440(10)°
C23H24Fe2Pd0.50Te2,F6P1,C2H3N
C23H24Fe2Pd0.50Te2,F6P1,C2H3N
Dalton transactions (Cambridge, England : 2003) (2006) 36 4335-4342
a=10.834(4)Å b=11.472(4)Å c=11.907(4)Å
α=79.70(3)° β=82.04(3)° γ=84.55(3)°
C23H24Fe2Pd0.50SeTe,F6P1,C2H3N
C23H24Fe2Pd0.50SeTe,F6P1,C2H3N
Dalton transactions (Cambridge, England : 2003) (2006) 36 4335-4342
a=10.923(3)Å b=11.701(4)Å c=11.860(4)Å
α=79.33(3)° β=73.42(3)° γ=86.88(3)°
C23H24Fe2Pt0.50Te2,F6P1,C2H3N
C23H24Fe2Pt0.50Te2,F6P1,C2H3N
Dalton transactions (Cambridge, England : 2003) (2006) 36 4335-4342
a=10.7920(10)Å b=11.4900(10)Å c=11.8650(10)Å
α=79.740(10)° β=82.180(10)° γ=84.500(10)°
C23H24Fe2Pt0.50SeTe,F6P,C2H3N
C23H24Fe2Pt0.50SeTe,F6P,C2H3N
Dalton transactions (Cambridge, England : 2003) (2006) 36 4335-4342
a=10.9230(10)Å b=11.6980(10)Å c=11.7910(10)Å
α=79.260(10)° β=73.240(10)° γ=86.670(10)°
C10H8N2
C10H8N2
Physical Chemistry Chemical Physics (2017)
a=13.842(7)Å b=9.396(4)Å c=7.518(3)Å
α=90° β=119.209(9)° γ=90°
C57.25H48.5Cl2.5Cu2Fe2I2Se4
C57.25H48.5Cl2.5Cu2Fe2I2Se4
RSC Adv. (2015)
a=22.7372(13)Å b=7.6135(4)Å c=32.6719(19)Å
α=90.00° β=90.00° γ=90.00°
C39H38Fe2NSe2
C39H38Fe2NSe2
RSC Adv. (2015)
a=10.7284(17)Å b=10.8211(17)Å c=16.282(2)Å
α=76.004(2)° β=73.266(2)° γ=65.170(2)°
C28H24FeSe2
C28H24FeSe2
RSC Adv. (2015)
a=27.419(8)Å b=6.0810(16)Å c=13.987(4)Å
α=90.00° β=107.285(3)° γ=90.00°
C79H76Cl2Cu4Fe4I4N2Se4
C79H76Cl2Cu4Fe4I4N2Se4
RSC Adv. (2015)
a=18.6299(10)Å b=15.4647(8)Å c=32.7558(14)Å
α=90.00° β=120.177(2)° γ=90.00°
C38H34Fe2Se2
C38H34Fe2Se2
RSC Adv. (2015)
a=5.8967(6)Å b=12.0644(13)Å c=42.577(5)Å
α=90.00° β=90.00° γ=90.00°
C84H68Cu2Fe2I2O4Se4
C84H68Cu2Fe2I2O4Se4
RSC Adv. (2015)
a=8.5325(12)Å b=14.3569(19)Å c=15.512(2)Å
α=85.587(2)° β=79.112(2)° γ=89.858(2)°
C84H68Br2Cu2Fe2O4Se4
C84H68Br2Cu2Fe2O4Se4
RSC Adv. (2015)
a=8.4445(11)Å b=14.2012(18)Å c=15.5454(19)Å
α=94.931(2)° β=102.002(2)° γ=90.115(2)°
2(C40H34Eu2O18),2(C1.50H3.50N0.50O0.50)
2(C40H34Eu2O18),2(C1.50H3.50N0.50O0.50)
CrystEngComm (2016) 18, 6 863
a=21.2904(4)Å b=21.2904(4)Å c=19.3576(7)Å
α=90.00° β=90.00° γ=90.00°
2(C40H34Gd2O18),2(C1.50H3.50N0.50O0.50)
2(C40H34Gd2O18),2(C1.50H3.50N0.50O0.50)
CrystEngComm (2016) 18, 6 863
a=21.2232(6)Å b=21.2232(6)Å c=19.3460(11)Å
α=90.00° β=90.00° γ=90.00°
2(C40H34Dy2O18),2(C1.50H3.50N0.50O0.50)
2(C40H34Dy2O18),2(C1.50H3.50N0.50O0.50)
CrystEngComm (2016) 18, 6 863
a=21.1619(9)Å b=21.1619(9)Å c=19.2599(15)Å
α=90.00° β=90.00° γ=90.00°
C29H26DyF12N5NiO10,H2O
C29H26DyF12N5NiO10,H2O
New J. Chem. (2015) 39, 5 3467
a=17.8522(18)Å b=10.6611(14)Å c=19.9365(12)Å
α=90° β=106.854(2)° γ=90°
C50H50Fe2N2O4Se4
C50H50Fe2N2O4Se4
Dalton transactions (Cambridge, England : 2003) (2018) 47, 5 1479-1487
a=26.224(6)Å b=5.9154(13)Å c=32.551(5)Å
α=90° β=113.754(13)° γ=90°
C15H20ClEu0NO6
C15H20ClEu0NO6
Dalton transactions (Cambridge, England : 2003) (2018) 47, 5 1479-1487
a=7.6294(18)Å b=33.347(8)Å c=7.1324(17)Å
α=90° β=110.008(3)° γ=90°
C27H28ClEu0FeN2O6Se2
C27H28ClEu0FeN2O6Se2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 5 1479-1487
a=10.880(4)Å b=11.998(5)Å c=21.837(8)Å
α=90° β=90° γ=90°
C25H25FeNO2Se2
C25H25FeNO2Se2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 5 1479-1487
a=8.9526(10)Å b=10.2338(11)Å c=24.890(3)Å
α=91.298(2)° β=94.727(2)° γ=93.742(2)°
C23H24Fe2Te2
C23H24Fe2Te2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 22 7463-7470
a=5.9310(12)Å b=10.639(2)Å c=35.440(7)Å
α=90.00° β=94.06(3)° γ=90.00°
C46H48Cu2Fe4I2Te4
C46H48Cu2Fe4I2Te4
Dalton transactions (Cambridge, England : 2003) (2018) 47, 22 7463-7470
a=10.5780(9)Å b=11.4374(10)Å c=11.7238(11)Å
α=100.572(3)° β=107.192(2)° γ=110.620(2)°
C28H26Fe2Te2
C28H26Fe2Te2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 22 7463-7470
a=20.7280(14)Å b=7.4755(5)Å c=17.1801(10)Å
α=90° β=102.440(2)° γ=90°
C28H26CuFe2ITe2
C28H26CuFe2ITe2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 22 7463-7470
a=9.440(9)Å b=9.571(9)Å c=15.338(15)Å
α=90.472(12)° β=90.454(13)° γ=94.755(12)°
C46H48Br2Cu2Fe4Te4
C46H48Br2Cu2Fe4Te4
Dalton transactions (Cambridge, England : 2003) (2018) 47, 22 7463-7470
a=10.623(2)Å b=11.340(3)Å c=12.013(3)Å
α=98.094(3)° β=113.331(2)° γ=110.988(2)°
C28H26BrCuFe2Te2
C28H26BrCuFe2Te2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 22 7463-7470
a=12.3650(6)Å b=10.8200(5)Å c=20.1765(9)Å
α=90° β=90.3880(10)° γ=90°
C28H26CuFe2ITe2
C28H26CuFe2ITe2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 22 7463-7470
a=12.4891(5)Å b=10.9033(5)Å c=20.1461(9)Å
α=90° β=90.8190(10)° γ=90°
C19H26AgFeSe4,PF6
C19H26AgFeSe4,PF6
Dalton transactions (Cambridge, England : 2003) (2010) 39, 37 8812-8819
a=6.9497(12)Å b=23.326(4)Å c=15.469(3)Å
α=90.00° β=93.971(2)° γ=90.00°
C19H26CuF6FePSe4
C19H26CuF6FePSe4
Dalton transactions (Cambridge, England : 2003) (2010) 39, 37 8812-8819
a=19.221(4)Å b=10.995(2)Å c=12.001(2)Å
α=90.00° β=90.00° γ=90.00°
C19H26FeSe4
C19H26FeSe4
Dalton transactions (Cambridge, England : 2003) (2010) 39, 37 8812-8819
a=20.9573(3)Å b=16.2170(2)Å c=6.1917(1)Å
α=90.00° β=90.00° γ=90.00°
C19H26FePdSe42,2(PF6)2
C19H26FePdSe42,2(PF6)2
Dalton transactions (Cambridge, England : 2003) (2010) 39, 37 8812-8819
a=10.0072(3)Å b=18.4143(4)Å c=15.9982(4)Å
α=90.00° β=106.850(3)° γ=90.00°
C19H26FePtSe42,2(PF6)2
C19H26FePtSe42,2(PF6)2
Dalton transactions (Cambridge, England : 2003) (2010) 39, 37 8812-8819
a=10.1013(4)Å b=18.6014(6)Å c=16.1256(6)Å
α=90.00° β=105.735(4)° γ=90.00°
C65H78ClDyN8Ni2O17.5
C65H78ClDyN8Ni2O17.5
Dalton transactions (Cambridge, England : 2003) (2016) 45, 26 10689-10695
a=13.256(6)Å b=15.998(7)Å c=17.783(8)Å
α=71.046(7)° β=88.592(7)° γ=68.988(6)°
C60H68DyN9Ni2O16
C60H68DyN9Ni2O16
Dalton transactions (Cambridge, England : 2003) (2016) 45, 26 10689-10695
a=13.3101(7)Å b=15.1304(8)Å c=17.5472(7)Å
α=73.642(2)° β=89.254(3)° γ=66.439(2)°
C60H68N9Ni2O16Tb
C60H68N9Ni2O16Tb
Dalton transactions (Cambridge, England : 2003) (2016) 45, 26 10689-10695
a=13.2669(7)Å b=15.1167(7)Å c=17.6076(10)Å
α=73.3906(17)° β=89.3892(19)° γ=66.6355(16)°
C60H68GdN9Ni2O16
C60H68GdN9Ni2O16
Dalton transactions (Cambridge, England : 2003) (2016) 45, 26 10689-10695
a=13.2375(6)Å b=15.1226(9)Å c=17.6501(10)Å
α=72.987(2)° β=89.432(3)° γ=66.867(2)°
C42H46Fe2N2Se4
C42H46Fe2N2Se4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3417-3428
a=26.243(3)Å b=5.8935(6)Å c=27.460(3)Å
α=90° β=112.9480(10)° γ=90°
C44H50Cl4Cu2Fe2I2N2Se4
C44H50Cl4Cu2Fe2I2N2Se4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3417-3428
a=10.4214(17)Å b=11.3687(18)Å c=12.1274(19)Å
α=117.235(2)° β=92.895(2)° γ=97.974(2)°
C46H52Br2Cu2Fe2N4Se4
C46H52Br2Cu2Fe2N4Se4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3417-3428
a=11.011(4)Å b=20.894(8)Å c=11.044(4)Å
α=90° β=110.632(6)° γ=90°
C21H23FeNSe2
C21H23FeNSe2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3417-3428
a=13.244(3)Å b=10.602(3)Å c=16.736(3)Å
α=90° β=125.019(12)° γ=90°
C44H54Cl2F12Fe2N2O2P2Pd2Se4
C44H54Cl2F12Fe2N2O2P2Pd2Se4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3417-3428
a=13.594(3)Å b=15.155(3)Å c=13.682(3)Å
α=90° β=108.069(2)° γ=90°
C44H52Cl2Cu2Fe2N2O10Se4
C44H52Cl2Cu2Fe2N2O10Se4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3417-3428
a=10.7820(5)Å b=19.2055(9)Å c=15.1526(5)Å
α=90° β=128.066(2)° γ=90°
C46H52Cu2F12Fe2N4P2Se4
C46H52Cu2F12Fe2N4P2Se4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 8 3417-3428
a=10.720(9)Å b=10.780(9)Å c=13.182(11)Å
α=105.674(10)° β=109.534(10)° γ=99.176(11)°
C28H26Fe2Se2
C28H26Fe2Se2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=15.997(18)Å b=5.781(7)Å c=13.752(15)Å
α=90° β=107.969(13)° γ=90°
C44H42Cu4Fe4I4N2Te4
C44H42Cu4Fe4I4N2Te4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=13.456(3)Å b=11.633(2)Å c=17.822(3)Å
α=90° β=95.547(2)° γ=90°
C21H20CuFe2ITe2
C21H20CuFe2ITe2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=7.4735(9)Å b=11.6218(14)Å c=13.8275(16)Å
α=104.7100(10)° β=100.6070(10)° γ=96.2980(10)°
C21H20CuFe2ISe2
C21H20CuFe2ISe2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=7.219(2)Å b=11.326(3)Å c=14.135(4)Å
α=106.724(3)° β=101.129(3)° γ=93.864(3)°
C21H20BrCuFe2Te2
C21H20BrCuFe2Te2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=7.532(3)Å b=11.313(4)Å c=13.866(5)Å
α=104.562(4)° β=101.494(4)° γ=96.643(4)°
C30H29Cu2Fe2I2NSe2
C30H29Cu2Fe2I2NSe2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=10.433(2)Å b=10.947(2)Å c=14.418(3)Å
α=104.744(3)° β=90.70(3)° γ=91.65(3)°
C21H20Cu2Fe2I2Se2
C21H20Cu2Fe2I2Se2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=16.987(6)Å b=16.987(6)Å c=16.186(11)Å
α=90° β=90° γ=90°
C20H20EuNO9
C20H20EuNO9
Dalton transactions (Cambridge, England : 2003) (2015) 44, 19 9281-9288
a=28.044(2)Å b=9.6262(7)Å c=8.2546(6)Å
α=90.00° β=90.00° γ=90.00°
C20H20GdNO9
C20H20GdNO9
Dalton transactions (Cambridge, England : 2003) (2015) 44, 19 9281-9288
a=28.017(3)Å b=9.6175(9)Å c=8.2586(7)Å
α=90.00° β=90.00° γ=90.00°
C20H20DyNO9
C20H20DyNO9
Dalton transactions (Cambridge, England : 2003) (2015) 44, 19 9281-9288
a=27.951(4)Å b=9.6124(13)Å c=8.1937(11)Å
α=90.00° β=90.00° γ=90.00°
<i>catena</i>-Poly[[[diaquanickel(II)]-bis[μ~2~-3-nitro-4-(pyridin-4-yl)benzoato-κ^2^<i>O</i>:<i>N</i>]] <i>N</i>,<i>N</i>-dimethylacetamide disolvate]
C24H18N4NiO10,2(C4H9NO)
Acta Crystallographica Section C (2019) 75, 2
a=11.866(7)Å b=12.259(7)Å c=14.248(14)Å
α=98.341(9)° β=93.604(9)° γ=117.018(6)°
Poly[[(μ~2~-acetato-κ^2^<i>O</i>:<i>O</i>)[μ~3~-3-nitro-4-(pyridin-4-yl)benzoato-κ^3^<i>O</i>:<i>O</i>':<i>N</i>]bis[μ~3~-3-nitro-4-(pyridin-4-yl)benzoato-κ^4^<i>O</i>,<i>O</i>':<i>O</i>':<i>N</i>]dicadmium(II)] <i>N</i>,<i>N</i>-dimethylacetamide disolvate monohydrate]
C38H24Cd2N6O14
Acta Crystallographica Section C (2019) 75, 2
a=8.342(4)Å b=13.903(6)Å c=23.568(10)Å
α=86.840(6)° β=89.264(6)° γ=78.826(6)°
Poly[[(<i>N</i>,<i>N</i>-dimethylformamide-κ<i>O</i>)bis[μ~2~-3-nitro-4-(pyridin-4-yl)benzoato-κ^3^<i>O</i>,<i>O</i>:<i>N</i>]cadmium(II)] <i>N</i>,<i>N</i>-dimethylformamide monosolvate methanol monosolvate]
C27H21CdN5O9
Acta Crystallographica Section C (2019) 75, 2
a=12.829(5)Å b=15.854(6)Å c=20.769(6)Å
α=90° β=122.215(18)° γ=90°
C28H30FeSe4
C28H30FeSe4
Inorganic Chemistry (2013) 52, 5786-5793
a=9.099(2)Å b=10.769(3)Å c=14.734(4)Å
α=73.561(4)° β=77.913(4)° γ=70.602(5)°
C30H35F12FeNOP2PdSe4
C30H35F12FeNOP2PdSe4
Inorganic Chemistry (2013) 52, 5786-5793
a=11.8549(13)Å b=13.1283(14)Å c=13.1835(14)Å
α=84.566(2)° β=67.686(2)° γ=80.060(2)°
C26H26FeS2Se2
C26H26FeS2Se2
Inorganic Chemistry (2013) 52, 5786-5793
a=19.220(12)Å b=11.524(7)Å c=21.878(14)Å
α=90.00° β=90.00° γ=90.00°
C26H26FeSe4
C26H26FeSe4
Inorganic Chemistry (2013) 52, 5786-5793
a=10.5443(16)Å b=14.235(2)Å c=31.750(5)Å
α=90.00° β=90.00° γ=90.00°
C26H26F12FeP2PdS2Se2
C26H26F12FeP2PdS2Se2
Inorganic Chemistry (2013) 52, 5786-5793
a=10.529(4)Å b=11.795(4)Å c=13.352(5)Å
α=75.373(4)° β=78.897(4)° γ=83.309(4)°
C26H26F12FeP2PtS2Se2
C26H26F12FeP2PtS2Se2
Inorganic Chemistry (2013) 52, 5786-5793
a=10.549(7)Å b=11.809(8)Å c=13.322(9)Å
α=75.320(8)° β=78.846(8)° γ=82.675(8)°
C21H19Fe2Se2
C21H19Fe2Se2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 3 1016-1024
a=24.338(5)Å b=7.4110(15)Å c=10.578(2)Å
α=90° β=90° γ=90°
C26H26F12FeP2PdSe4
C26H26F12FeP2PdSe4
Inorganic Chemistry (2013) 52, 5786-5793
a=10.6758(19)Å b=11.868(2)Å c=13.387(2)Å
α=75.271(3)° β=78.638(3)° γ=83.311(3)°